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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1615104Generated: November 2, 2026

HCID 178502340, compound → HCID 178502341, compound

https://huagongshe.com/reaction/1615104

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178502340HCID 178502340—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 178502341HCID 17850234159.5%

Reaction Steps

To a solution of compound from example 19 (15 mg) in 3 mL of methanol is added Pd—C 10% (5 mg). The reaction is stirred for 30 minutes under hydrogen atmosphere. The reaction mixture is filtered, concentrated to dryness and the residue is purified by reverse phase HPLC to give title compound as a white solid (8 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765731B2
Source datasetuspto-grants-2014_07
ORD IDord-b6f7795d2fac45f99d151fee6afab2b7
Source noteuspto-grants-2014_07