HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178502340, compound → HCID 178502341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178502340 | HCID 178502340 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178502341 | HCID 178502341 | 59.5% |
Reaction Steps
To a solution of compound from example 19 (15 mg) in 3 mL of methanol is added Pd—C 10% (5 mg). The reaction is stirred for 30 minutes under hydrogen atmosphere. The reaction mixture is filtered, concentrated to dryness and the residue is purified by reverse phase HPLC to give title compound as a white solid (8 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765731B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-b6f7795d2fac45f99d151fee6afab2b7 |
| Source note | uspto-grants-2014_07 |