Allyl bromide → HCID 67995672, compound

HRID 1615116Notes

Reaction equation

HRID 1615116 reaction equation
[CH3:1][C:2]1([CH3:14])[CH2:7][O:6][C:5]2([CH2:12][CH2:11][C:10](=[O:13])[CH2:9][CH2:8]2)[O:4][CH2:3]1.[CH2:15](Br)[CH:16]=[CH2:17]>>[CH2:17]([C:10]1([OH:13])[CH2:11][CH2:12][C:5]2([O:4][CH2:3][C:2]([CH3:14])([CH3:1])[CH2:7][O:6]2)[CH2:8][CH2:9]1)[CH:16]=[CH2:15]

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 5879683,3-Dimethyl-1,5-dioxaspiro(5.5)undecan-9-one

Product 1

HCID 67995672HCID 67995672, compound

Procedure

The title compound is prepared from 3,3-dimethyl-1,5-dioxa-spiro[5.5]undecan-9-one and allyl bromide following a procedure analogous to that described in Step 1 of Intermediate 2. Yield: quantitative; Mass spectrum (ESI+): m/z=223 [M+H—H2O]+.

Sources & evidence

ORD record
ord-e2f5f29519334d74b1f696cdea622bd4
Source dataset
uspto-grants-2014_07
Patent number
US08765744B2

Reaction notes

Loading…