HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 10703113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 1,4-Dioxaspiro[4.5]decan-7-one | HCID 240602 | — |
| Product | HCID 10703113 | HCID 10703113 | 84% |
Reaction Steps
The title compound is prepared from 1,4-dioxa-spiro[4.5]decan-7-one and allyl bromide following a procedure analogous to that described in Step 1 of Intermediate 2. Yield: 84% of theory; Mass spectrum (ESI+): m/z=181 [M+H—H2O]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e61daed4c9604d74bbc7dcf51a112b28 |
| Source note | uspto-grants-2014_07 |