HuagongsheHuagongshe Chemistry Print Report · For research reference only
(alphaS)-4-Bromo-alpha-methylbenzenemethanamine → HCID 67995969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (alphaS)-4-Bromo-alpha-methylbenzenemethanamine | HCID 852999 | — |
| Reactant | HCID 11694101 | HCID 11694101 | — |
| Product | HCID 67995969 | HCID 67995969 | 68% |
Reaction Steps
The title compound is prepared from (7-hydroxy-1,4-dioxa-spiro[4.5]dec-7-yl)-acetaldehyde and (S)-1-(4-bromo-phenyl)-ethylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 68% of theory; LC (method 1): tR=3.83 min; Mass spectrum (ESI+): m/z=384/386 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-cb65c8f8e1fd48b9ad3778a00b6ab55c |
| Source note | uspto-grants-2014_07 |