Allyl bromide → HCID 67995979, compound

HRID 1615127Notes

Reaction equation

[OH:1][C:2]12[CH2:11][CH:6]3[CH2:7][CH:8]([CH2:10][CH:4]([C:5]3=[O:12])[CH2:3]1)[CH2:9]2.[CH2:13](Br)[CH:14]=[CH2:15]>>[CH2:15]([C:5]1([OH:12])[CH:6]2[CH2:11][C:2]3([OH:1])[CH2:9][CH:8]([CH2:10][CH:4]1[CH2:3]3)[CH2:7]2)[CH:14]=[CH2:13]

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 64184Idramantone

Product 1

HCID 67995979HCID 67995979, compound

Procedure

The title compound is prepared from 5-hydroxy-adamantan-2-one and allyl bromide following a procedure analogous to that described in Step 1 of Intermediate 2. Yield: quantitative; Mass spectrum (ESI+): m/z=226 [M+NH4]+.

Sources & evidence

ORD record: ord-9798f01a431447a1a2be2c8ee76c517e
Source dataset: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08765744B2

Reaction notes

Loading…