Allyl bromide → HCID 67995858, compound

HRID 1615130Notes

Reaction equation

[CH2:1]([O:3][C:4]([CH:6]1[CH2:11][CH2:10][C:9](=[O:12])[CH2:8][CH2:7]1)=[O:5])[CH3:2].[CH2:13](Br)[CH:14]=[CH2:15]>>[CH2:1]([O:3][C:4]([CH:6]1[CH2:11][CH2:10][C:9]([CH2:15][CH:14]=[CH2:13])([OH:12])[CH2:8][CH2:7]1)=[O:5])[CH3:2]

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 317638Ethyl 4-oxocyclohexanecarboxylate

Product 1

HCID 67995858HCID 67995858, compound

Procedure

The title compound is prepared from 4-oxo-cyclohexanecarboxylic acid ethyl ester and allyl bromide following a procedure analogous to that described in Step 1 of Intermediate 2. Yield: quantitative; Mass spectrum (ESI+): m/z=213 [M+H]+.

Sources & evidence

ORD record: ord-891f49a57c734cc6a082bf3ce3b794ab
Source dataset: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08765744B2

Reaction notes

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