(S)-1-(2,4-Difluorophenyl)ethanamine → HCID 67995737, compound

Participants

Reaction Steps

The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-(2,4-difluoro-phenyl)-ethylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 66% of theory; LC (method 5): tR=0.99 min; Mass spectrum (ESI+): m/z=384 [M+H]+.

Provenance & Evidence