HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (-)- → HCID 67996181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Reactant | (9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde | HCID 86668369 | — |
| Product | HCID 67996181 | HCID 67996181 | 62% |
Reaction Steps
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-phenyl-ethylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 62% of theory; LC (method 6): tR=1.10 min; Mass spectrum (ESI+): m/z=348 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-48b0813344f6485590685a3b00a543c5 |
| Source note | uspto-grants-2014_07 |