Triphosgene → HCID 70497137, compound

Participants

Reaction Steps

The title compound is prepared from N-(8-{2-[(S)-1-(4-chloro-phenyl)-ethylamino]-ethyl}-1,4-dioxa-spiro[4.5]dec-8-yl)-2,2,2-trifluoro-acetamide and triphosgene following a procedure analogous to that described in Step 4 of Intermediate 2. Yield: quantitative (crude); Mass spectrum (ESI+): m/z=365/367 (Cl) [M+H]+.

Provenance & Evidence