5-Bromo-2-oxindole → HCID 178517023, compound

Participants

Reaction Steps

The title compound was synthesized according to the method described for Example A1, except reacting 5-bromooxindole (39 mg, 0.185 mmol) with 1H-benzo[d][1,2,3]triazole-5-carbaldehyde (30 mg, 0.204 mmol) to obtain 32 mg, 51%. 1H NMR (400 MHz, d6-DMSO) δ 15.97 (s, 1H), 10.85 (s, 1H), 9.27 (s, 1H), 8.37 (d, J=9.2 Hz, 1H), 8.16 (s, 1H), 8.02 (s, 1H), 7.95 (d, J=8.4 Hz, 1H), 7.39 (d, J=8.2 Hz, 1H), 6.80 (d, J=8.3 Hz, 1H); MS ESI 341.0 [M+H]+, calcd for [C15H9BrN4O+H]+ 341.00.

Provenance & Evidence