6-Chloro-1,3-dihydroindol-2-one → HCID 178517232, compound

Participants

Reaction Steps

The title compound was synthesized according to the method described for Example A1 except reacting 6-chlorooxindole (36 mg, 0.216 mmol) with 1H-benzo[d][1,2,3]triazole-5-carbaldehyde (35 mg, 0.238 mmol) to obtain 32 mg, 51%. 1H NMR (400 MHz, d6-DMSO) δ 15.95 (s, 1H), 10.81 (s, 1H), 8.27 (bs, 1H), 8.04 (bs, 1H), 7.85 (s, 1H), 7.76 (bs, 1H), 7.49 (d, J=8.8 Hz, 1H), 6.91 (bs, 2H); MS ESI 297.0 [M+H]+, calcd for [C15H9ClN4O+H]+ 297.05.

Provenance & Evidence