HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Oxoindolin-6-yl)acetamide → HCID 178474027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Oxoindolin-6-yl)acetamide | HCID 2749839 | — |
| Reactant | HCID 178519388 | HCID 178519388 | — |
| Product | HCID 178474027 | HCID 178474027 | — |
Reaction Steps
The title compound was synthesized according to the method described for Example A11B except substituting N-(2-oxoindolin-6-yl)acetamide (30 mg, 0.158 mmol) and 1H-benzo[d][1,2,3]triazole-6-carbaldehyde (26 mg, 0.174 mmol) to obtain 22 mg, 44%. 1H NMR (400 MHz, d6-DMSO) δ ˜16 (s, 1H), 10.60 (s, 1H), 10.10 (s, 1H), 8.23 (s, 1H), 8.01 (s, 1H), 7.73 (d, J=8.0 Hz, 1H), 7.64 (s, 1H), 7.51 (s, 1H), 7.47 (d, J=8.0 Hz, 1H), 6.86 (d, J=7.4 Hz, 1H), 2.02 (s, 3H); MS ESI 320.1 [M+H]+, calcd for [C17H13N5O2+H]+ 320.11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-4a3673af7fba483c90b8599ad119e0ee |
| Source note | uspto-grants-2014_07 |