HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Oxoindolin-6-yl)acetamide → HCID 178474026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Oxoindolin-6-yl)acetamide | HCID 2749839 | — |
| Reactant | 1H-Indazole-5-carboxaldehyde | HCID 21250644 | — |
| Product | HCID 178474026 | HCID 178474026 | — |
Reaction Steps
The title compound was synthesized according to the method described for Example A11B except substituting N-(2-oxoindolin-6-yl)acetamide (40 mg, 0.210 mmol) and 1H-indazole-5-carbaldehyde (34 mg, 0.231 mmol) to obtain 41 mg, 61%. 1H NMR (400 MHz, d6-DMSO) δ 13.31 (s, 1H), 10.55 (s, 1H), 10.07 (s, 1H), 8.19 (s, 1H), 8.15 (s, 1H), 7.71-7.64 (m, 2H), 7.61 (s, 1H), 7.57 (d, J=8.4 Hz, 1H), 7.48 (s, 1H), 6.89 (d, J=8.3 Hz, 1H), 2.04 (s, 3H); MS ESI 319.1 [M+H]+, calcd for [C18H14N4O2+H]+ 319.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-95a3b5cb5ee34cef82b06d781e026b6b |
| Source note | uspto-grants-2014_07 |