HCID 45582882, compound → HCID 178457913, compound

Participants

Reaction Steps

According to the method of Example A20, except substituting 1-isopropyl-3-(2-oxoindolin-5-yl)urea (23 mg, 0.099 mmol) and 1H-benzo[d][1,2,3]triazole-5-carbaldehyde (15 mg, 0.11 mmol), the title compound was obtained as an orange solid (6 mg, 16%). 1H NMR (400 MHz, DMSO-d6) δ 10.44 (s, 1H), 8.01 (s 1H), 7.75 (s, 1H), 7.57-7.59 (m, 2H), 7.31 (d, J=7.6 Hz, 1H), 6.74 (d, J=8.4 Hz, 1H), 5.76 (d, J=7.6 Hz, 1H), 3.75-3.70 (m, 1H), 1.03-1.00 (d, 6H); MS ESI 363.1 [M+H]+, calcd for [C20H19N5O2+H]+ 363.2.

Provenance & Evidence