HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-oxindole → HCID 178517021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-oxindole | HCID 611193 | — |
| Reactant | 1H-Indazole-6-carbaldehyde | HCID 18538368 | — |
| Product | HCID 178517021 | HCID 178517021 | — |
Reaction Steps
The title compound was synthesized according to the method described for Example A11B except substituting 5-bromooxindole (40 mg, 0.189 mmol) and 1H-indazole-6-carbaldehyde (30 mg, 0.208 mmol) to obtain 1.0 mg (1.6%) of a yellow solid. 1H NMR (400 MHz, CD3OD) δ 8.16 (s, 1H), 7.98-7.92 (m, 2H), 7.87 (s, 1H), 7.73 (s, 1H), 7.44 (d, J=8.34 Hz, 1H), 7.39 (d, J=8.59 Hz, 1H), 6.87 (d, J=8.34 Hz, 1H); MS ESI 340.1 [M+H]+, calcd for [C16H10BrN3O+H]+ 340.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-a908f5c2c7a447b19a7839e4ddd3c734 |
| Source note | uspto-grants-2014_07 |