HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxindole → HCID 178517069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxindole | HCID 321710 | — |
| Reactant | HCID 76846386 | HCID 76846386 | — |
| Product | HCID 178517069 | HCID 178517069 | 16.9% |
Reaction Steps
The compound was synthesized according to the method described for Example A1. Oxindole (8 mg, 0.06 mmol) was reacted with 4-chloro-1H-indazole-6-carbaldehyde (11 mg, 0.06 mmol) to give the title compound as an orange solid (3 mg, 13%). 1H NMR (400 MHz, CD3OD) δ 8.21 (s, 1H), 7.87 (s, 1H), 7.82 (s, 1H), 7.59 (d, 1H, J=7.8 Hz), 7.48 (s, 1H), 7.28 (t, 1H, J=7.9 Hz), 6.95 (d, 1H, J=7.7 Hz), 6.90 (t, 1H, J=8.2 Hz); MS ESI [M+H]+, calcd for [C16H10ClN3O+H]+ 296.1; found m/z 296.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-5c03229ca40142718b0fdc215ded270f |
| Source note | uspto-grants-2014_07 |