HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 68758903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | 4-Bromo-1H-indazole-6-carboxylic acid | HCID 24728402 | — |
| Product | HCID 68758903 | HCID 68758903 | 88.1% |
Reaction Steps
According to the method of A52A, 4-bromo-1H-indazole-6-carboxylic acid (1 g, 4 mmol) was reacted with borane (6 ml, 6 mmol) to give the title compound as a pale yellow solid (800 mg, 88%). MS ESI [M+H]+, calcd for [C8H7BrN2O+H]+ 227.0, 229.0; found m/z 226.9, 228.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-b8e0bffa1cd745469a7fa3e015c4ab7f |
| Source note | uspto-grants-2014_07 |