HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cornforth reagent → 4-bromo-1H-indazole-6-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cornforth reagent | HCID 2724130 | — |
| Reactant | HCID 68758903 | HCID 68758903 | — |
| Product | 4-bromo-1H-indazole-6-carbaldehyde | HCID 59635585 | 53% |
Reaction Steps
According to the method of A52B, (4-bromo-1H-indazol-6-yl)methanol was oxidized with PDC to give the title compound as a beige solid (413 mg, 53%). MS ESI [M+H]+, calcd for [C8H5BrN2O+H]+ 225.0, 227.0; found m/z 224.9, 226.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-1732fb0f1ad84beb8d0fdd70987f1471 |
| Source note | uspto-grants-2014_07 |