HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxindole → HCID 68754821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxindole | HCID 321710 | — |
| Reactant | HCID 86651996 | HCID 86651996 | — |
| Product | HCID 68754821 | HCID 68754821 | — |
Reaction Steps
According to the method of A57B, oxindole (39 mg, 0.29 mmol) was reacted (E)-3-(4-(morpholinomethyl)styryl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-indazole-6-carbaldehyde (116 mg, 0.25 mmol) to give the title compound as a yellow solid upon silica gel purification (95:5 CH2Cl2/MeOH) (95 mg, 64%). MS ESI 593.5 [M+H]+, calcd for [C35H40N4O3Si+H]+ 593.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-20a158824c094f3fb8e64ea2259bdb90 |
| Source note | uspto-grants-2014_07 |