Water → HCID 58159630, compound

Participants

Reaction Steps

Sodium hydride (60% in mineral oil, 40 mg, 0.98 mmol) was added at room temperature to a mixture solution of 6-(3-nitrophenyl)-1H-indole (117 mg, 0.49 mmol) in DMF (2 mL). 10 minutes later, 4-chloro-2-(methylthio)pyrimidine (68 μL, 0.59 mmol) was added. After stirring at room temperature for 30 minutes, water was added. Thus prepared solid was filtered and dried. The target compound (102 mg) was yielded as white solid.

Provenance & Evidence