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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1615691Generated: November 3, 2026

HCID 178500432, compound → HCID 68089282, compound

https://huagongshe.com/reaction/1615691

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178500432HCID 178500432—
SolventAcetic AcidHCID 176—
ProductHCID 68089282HCID 68089282111.9%

Reaction Steps

A solution of (Z)-methyl-4-(1-amino-3,6-dimethylpyrazin-2(1H)-ylideneamino)-3-methyl-4-oxobutanoate (1.10 g, 4.14 mmol) in acetic acid (15 mL) was stirred at 140° C. for 2 h in a microwave reactor. The solution was evaporated to give 1.15 g of the product as a brown solid. ESI MS: m/z 248 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765760B2
Source datasetuspto-grants-2014_07
ORD IDord-02d5f196ee6b445da5aca154b2c541f7
Source noteuspto-grants-2014_07