HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178500432, compound → HCID 68089282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178500432 | HCID 178500432 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68089282 | HCID 68089282 | 111.9% |
Reaction Steps
A solution of (Z)-methyl-4-(1-amino-3,6-dimethylpyrazin-2(1H)-ylideneamino)-3-methyl-4-oxobutanoate (1.10 g, 4.14 mmol) in acetic acid (15 mL) was stirred at 140° C. for 2 h in a microwave reactor. The solution was evaporated to give 1.15 g of the product as a brown solid. ESI MS: m/z 248 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765760B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-02d5f196ee6b445da5aca154b2c541f7 |
| Source note | uspto-grants-2014_07 |