HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Oxaspiro[5.5]undec-7-en-9-one → 3-Oxaspiro[5.5]undecan-9-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Oxaspiro[5.5]undec-7-en-9-one | HCID 68763689 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Oxaspiro[5.5]undecan-9-one | HCID 68765783 | — |
Reaction Steps
Under a hydrogen atmosphere 1.30 g (7.82 mmol) 3-oxaspiro[5.5]undec-7-en-9-one were hydrogenated with 0.2 g Pd/C (10%) in 15 ml of ethyl acetate at 50° C. and 3 bar hydrogen pressure for three days. The reaction mixture was suction filtered and evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765763B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d71340bca72e442c982bd127c0715c99 |
| Source note | uspto-grants-2014_07 |