HCID 86691849, compound → HCID 86691850, compound

Participants

Reaction Steps

To a solution of 42-1 (1.4 g, 3.6 mmol) in EtOH (9 mL) was added 10% Pd/C (500 mg) and the flask was purged with hydrogen and fitted with a balloon filled with hydrogen gas. After 15 hours, the solution was filtered, concentrated and purified by reverse phase chromatography (1-100% Acetonitrile, 0.1% TFA in H2O) and the desired fractions were concentrated to give product. MS (M+H)+: observed=367.2, calculated=367.5.

Provenance & Evidence