HRID1616911

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)OC(=O)N1CCc2c(oc3cc(I)ccc23)C1

HCID67323433

未命名化合物

HCID67324003

2-(6-Iodo-1-benzofuran-3-yl)ethan-1-amine--hydrogen chloride (1/1)

C10H11ClINO

PRODUCTS

生成物

HCID68304680

未命名化合物

PROCEDURE

实验过程

Synthesized as described for tert-butyl 7-iodo-3,4-dihydro[1]benzofuro[2,3-c]pyridine-2(1H)-carboxylate starting from 2-(6-iodo-1-benzofuran-3-yl)ethanamine hydrochloride. MS m/z 332 [M+H]+. 1H-NMR (400 MHz, CDCl3): δ 1.43 (s, 9H), 2.85 (t, 2H), 3.43 (q, 2H), 4.62 (bs, 1H), 7.31 (d, 1H), 7.39 (s, 1H), 7.54 (dd, 1H), 7.84 (d, 1H).

WORKUP

后处理

customSynthesized