HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → 7-Iodo-1-methyl-1,2,3,4-tetrahydro[1]benzofuro[2,3-c]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 7-Iodo-1,2,3,4-tetrahydro[1]benzofuro[2,3-c]pyridine | HCID 67324876 | — |
| Product | 7-Iodo-1-methyl-1,2,3,4-tetrahydro[1]benzofuro[2,3-c]pyridine | HCID 67323371 | — |
Reaction Steps
Synthesized as described for 7-iodo-1,2,3,4-tetrahydro[1]benzofuro[2,3-c]pyridine using acetaldehyde. 1H-NMR (400 MHz, CDCl3): δ 1.60 (d, 3H), 2.92 (m, 2H), 3.37 (m, 1H), 3.59 (m, 1H), 4.77 (m, 1H), 7.46 (d, 1H), 7.64 (dd, 1H), 8.07 (d, 1H), 9.58 (bs, 1H), 10.02 (bs, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765779B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e6d76b0c52b04b57af2a5c5ce776e22f |
| Source note | uspto-grants-2014_07 |