HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-Iodosalicylate → 2-(5-Iodo-1-benzofuran-3-yl)ethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-Iodosalicylate | HCID 248910 | — |
| Reactant | 2-(6-Iodo-benzofuran-3-yl)-ethylamine | HCID 67324004 | — |
| Product | 2-(5-Iodo-1-benzofuran-3-yl)ethanamine | HCID 67325332 | — |
Reaction Steps
Synthesized as described for 2-(6-iodo-1-benzofuran-3-yl)ethanamine using methyl 2-hydroxy-5-iodobenzoate. 1H-NMR (400 MHz, DMSO-d6): δ 2.91 (t, J=7.7 Hz, 2H), 3.11 (m, 2H), 7.45 (d, J=8.5 Hz, 1H), 7.65 (dd, J=8.5, 1.8 Hz, 1H), 7.90 (s, 1H), 8.09 (bs, 2H), 8.11 (d, J=1.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765779B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e4e3278eab1c4339afbcaf170538823b |
| Source note | uspto-grants-2014_07 |