HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5-Iodo-1-benzofuran-3-yl)ethanamine → Tert-butyl[2-(5-iodo-1-benzofuran-3-yl)ethyl]carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5-Iodo-1-benzofuran-3-yl)ethanamine | HCID 67325332 | — |
| Reactant | Tert-butyl[2-(6-iodo-1-benzofuran-3-yl)ethyl]carbamate | HCID 68304680 | — |
| Product | Tert-butyl[2-(5-iodo-1-benzofuran-3-yl)ethyl]carbamate | HCID 68305709 | — |
Reaction Steps
Synthesized as described for tert-butyl[2-(6-iodo-1-benzofuran-3-yl)ethyl]carbamate using 2-(5-iodo-1-benzofuran-3-yl)ethanamine. 1H-NMR (400 MHz, CDCl3): δ 1.44 (s, 9H), 2.84 (t, 1H), 3.43 (q, 2H), 4.62 (bs, 1H), 7.25 (d, 1H), 7.43 (s, 1H), 7.56 (dd, 1H), 7.88 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765779B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d66f2a8ceb7241ec9662c68bec0df2fe |
| Source note | uspto-grants-2014_07 |