HCID 53327613, compound → HCID 67375002, compound

HRID 1616948Notes

Reaction equation

C(OC(N1CCC2C3C=CC(S(C4C=CC=C(O)C=4)(=O)=O)=CC=3OC2C1)=O)(C)(C)C.[C:31]([O:35][C:36]([N:38]1[CH2:43][CH2:42][CH:41]2[C:44]3[CH:50]=[CH:49][C:48]([S:51]([C:54]4[CH:59]=[C:58]([O:60][CH:61]([CH3:63])[CH3:62])[CH:57]=[C:56]([O:64]CC5C=CC=CC=5)[CH:55]=4)(=[O:53])=[O:52])=[CH:47][C:45]=3[O:46][CH:40]2[CH2:39]1)=[O:37])([CH3:34])([CH3:33])[CH3:32]>>[C:31]([O:35][C:36]([N:38]1[CH2:43][CH2:42][CH:41]2[C:44]3[CH:50]=[CH:49][C:48]([S:51]([C:54]4[CH:59]=[C:58]([O:60][CH:61]([CH3:62])[CH3:63])[CH:57]=[C:56]([OH:64])[CH:55]=4)(=[O:53])=[O:52])=[CH:47][C:45]=3[O:46][CH:40]2[CH2:39]1)=[O:37])([CH3:34])([CH3:33])[CH3:32]

Participants

Reactant 2

HCID 53327613HCID 53327613, compound

HCID 67325455HCID 67325455, compound

Product 1

HCID 67375002HCID 67375002, compound

Procedure

Synthesized as described for 7-(3-Hydroxy-benzenesulfonyl)-3,4,4a,9a-tetrahydro-1H-benzo[4,5]furo[2,3-c]pyridine-2-carboxylic acid tert-butyl ester D01 starting from 7-(3-benzyloxy-5-isopropoxy-benzenesulfonyl)-3,4,4a,9a-tetrahydro-1H-benzo[4,5]furo[2,3-c]pyridine-2-carboxylic acid tert-butyl ester.

Workup

customSynthesized

Sources & evidence

ORD record: ord-8cf633c82302405ebd4a84545e1e7310
Source dataset: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08765779B2

Reaction notes

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