HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-(1-(2-Methoxyethyl)piperidin-4-ylidene)acetyl chloride hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(1-(2-Methoxyethyl)piperidin-4-ylidene)acetic acid | HCID 59382660 | — |
| Product | 2-(1-(2-Methoxyethyl)piperidin-4-ylidene)acetyl chloride hydrochloride | HCID 86629758 | — |
Reaction Steps
2.4 g of 2-(1-(2-methoxyethyl)piperidin-4-ylidene)acetic acid was dissolved in 20 mL of thionyl chloride, refluxed for 2 hours, evaporated in vacuo to remove thionyl chloride and give a solid product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765946B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c1b268ae301e417990aa25469425606d |
| Source note | uspto-grants-2014_07 |