Isopropanol → HCID 136385607, compound

Participants

Reaction Steps

As a byproduct from the crude reaction mixture of example 12, step 2, HPLC separation (Chiralpak AD column, 10% isopropanol in n-heptane) provided 3-(3-bromo-phenyl)-1-pyridin-4-yl-pentan-1-one oxime as a mixture of E and Z isomers (4:1) as a colorless oil, MS (ESI+): m/z=333.0 ([M+H]+, 1Br).

Provenance & Evidence