6-(Methoxycarbonyl)pyridine-3-boronic acid → HCID 66666146, compound

Participants

Reaction Steps

In analogy to example 74, step 6, from 3-(3-bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one (example 98, step 5) and 2-(methylcarboxy)pyridine-5-boronic acid (4 h at 80° C., 40 h at rt) was prepared the title compound as an off-white semisolid, MS (ESI−): m/z=435.2 ([M−H]−, 1Br).

Provenance & Evidence