HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Carboxyphenylboronic acid → 3'-[3-(2-Methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-biphenyl-3-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Carboxyphenylboronic acid | HCID 2733957 | — |
| Reactant | HCID 67015516 | HCID 67015516 | — |
| Product | 3'-[3-(2-Methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-biphenyl-3-carboxylic acid | HCID 66666549 | — |
Reaction Steps
In analogy to example 74, step 6, from 3-(3-bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one (example 98, step 5) and 3-carboxyphenylboronic acid was prepared the title compound as an off-white solid, MS (ESI−): m/z=434.3 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c0223fde79624b398003077bc454e639 |
| Source note | uspto-grants-2014_07 |