HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxycarbonylphenylboronic acid → 3'-[3-(2-Methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-biphenyl-4-carboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxycarbonylphenylboronic acid | HCID 2734369 | — |
| Reactant | HCID 67015516 | HCID 67015516 | — |
| Product | 3'-[3-(2-Methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-biphenyl-4-carboxylic acid methyl ester | HCID 66669270 | — |
Reaction Steps
In analogy to example 19, from 3-(3-bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one (example 98, step 5) and 4-methoxycarbonyl-phenylboronic acid was prepared the title compound as a yellow foam, MS (ESI+): m/z=450.3 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-9dfe1678a2aa4be69e239c6e2cc38fd1 |
| Source note | uspto-grants-2014_07 |