Hydroxyamine hydrochloride → HCID 136360006, compound

Participants

Reaction Steps

In analogy to example 74, step 7, from 5-{4-[3-(2-methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-phenyl}-pent-4-ynoic acid and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (4.2:1) as a colorless oil, MS (ESI−): m/z=425.1862 ([M−H]−).

Provenance & Evidence