Hydroxyamine hydrochloride → HCID 136360007, compound

Participants

Reaction Steps

In analogy to example 74, step 7, from 3-fluoro-4′-[3-(2-methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-biphenyl-4-carboxylic acid and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (5.8:1) as a colorless oil, MS (ESI+): m/z=469.1917 ([M+H]+).

Provenance & Evidence