Hydroxyamine hydrochloride → HCID 136166844, compound

Participants

Reaction Steps

In analogy to example 74, step 7, from 3-(4-bromo-phenyl)-3-(3-methyl-pyridin-2-yl)-1-(2-methyl-pyridin-4-yl)-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound which contains less than 6% of the Z isomer as a colorless oil, MS (ESI+): m/z=410.0872 ([M+H]+, 1Br).

Provenance & Evidence