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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617594Generated: November 3, 2026

Hydroxyamine hydrochloride → HCID 136167067, compound

https://huagongshe.com/reaction/1617594

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66667223HCID 66667223—
ProductHCID 136167067HCID 136167067—

Reaction Steps

In analogy to example 74, step 7, from 3-(4-bromophenyl)-3-(4-chloro-2-methylphenyl)-1-(2-methylpyridin-4-yl)propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound which contains less than 10% of the Z isomer as a white foam, MS (ESI+): m/z=445.05 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-8fbf61a020284481889576040e13de2d
Source noteuspto-grants-2014_07