HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methylpyridine → (R)-3-(4-Bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methylpyridine | HCID 2762835 | — |
| Reactant | (R)-3-(4-Bromophenyl)-N-methoxy-N-methyl-3-o-tolylpropanamide | HCID 71813344 | — |
| Product | (R)-3-(4-Bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one | HCID 66666695 | — |
Reaction Steps
In analogy to example 74, step 5, from (R)-3-(4-bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide and 4-bromo-2-methylpyridine was prepared the title compound as yellow solid, MS (ESI+): m/z=394.0797 ([M+H]+, 1Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d27f3dbc6d1145f8a3dbe24ab85cea1d |
| Source note | uspto-grants-2014_07 |