HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dimethylanisole → HCID 67015706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dimethylanisole | HCID 278654 | — |
| Reactant | 3-(4-Bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide | HCID 86660949 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 67015706 | HCID 67015706 | — |
Reaction Steps
In analogy to example 151, step 1, 4-bromo-2,6-dimethylanisole was reacted first with n-butyllithium and later with 3-(4-bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide (example 74, step 4) to give the title compound as a light yellow solid, MS (ESI+): m/z=437.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ee77de684f584260bcb97ad882bec80d |
| Source note | uspto-grants-2014_07 |