HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methylpyridine → HCID 67015629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methylpyridine | HCID 2762835 | — |
| Reactant | HCID 86661015 | HCID 86661015 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 67015629 | HCID 67015629 | — |
Reaction Steps
In analogy to example 151, step 1, 4-bromo-2-methylpyridine was reacted first with n-butyllithium and later with N-methoxy-2-[1-(4-methoxy-phenyl)-cyclohexyl]-N-methyl-acetamide to give the title compound as a light yellow oil, MS (ESI+): m/z=324.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-f81e198255c249c6828772437d7d76b0 |
| Source note | uspto-grants-2014_07 |