HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67015599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67015533 | HCID 67015533 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67015599 | HCID 67015599 | — |
Reaction Steps
In analogy to example 162, step 2, 3-(4-bromo-phenyl)-7,7,7-trifluoro-1-(6-methoxy-pyridin-3-yl)-heptan-1-one was reacted with concentrated aqueous HCl in 1,4-dioxane to give the title compound as a light yellow oil, MS (ESI+): m/z=416.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-09fbdbf2993849138935ea4fd3ff6a5d |
| Source note | uspto-grants-2014_07 |