Hydrochloric Acid → HCID 67015550, compound

Participants

Reaction Steps

In analogy to example 151, step 1, 5-bromo-2-methoxy-4-methylpyridine was reacted first with n-butyllithium and later with 3-(4-bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide (example 74, step 4). The product of this reaction was reacted with concentrated aqueous HCl in 1,4-dioxane in analogy to example 162, step 2 to give the title compound as a colorless foam, MS (ESI+): m/z=410.2 [M+H]+.

Provenance & Evidence