HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-methoxypyridine → HCID 67015636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-methoxypyridine | HCID 2734895 | — |
| Reactant | HCID 86661001 | HCID 86661001 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 67015636 | HCID 67015636 | — |
Reaction Steps
In analogy to example 151, step 1, 5-bromo-2-methoxypyridine was reacted first with n-butyllithium and later with 3-(4-bromophenyl)-3-(4-fluoro-2-methylphenyl)-N-methoxy-N-methylpropanamide (example 141, step 3) to give the title compound as a light yellow oil, MS (ESI+): m/z=430.06 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-6b58cb82c0064073bccf8c21d68ad8ed |
| Source note | uspto-grants-2014_07 |