HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methylpyridine → (S)-3-(4-Bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methylpyridine | HCID 2762835 | — |
| Reactant | (S)-3-(4-bromophenyl)-N-methoxy-N-methyl-3-o-tolylpropanamide | HCID 71813343 | — |
| Product | (S)-3-(4-Bromo-phenyl)-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one | HCID 67015671 | — |
Reaction Steps
In analogy to example 74, step 5, from (S)-3-(4-bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide (example 142, step 1) and 4-bromo-2-methylpyridine was prepared the title compound as white solid, MS (ESI+): m/z=394.0 ([M+H]+, 1Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-0553ae5e7b9747c8ba0bba29b7cf4bcd |
| Source note | uspto-grants-2014_07 |