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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617912Generated: November 3, 2026

Hydroxyamine hydrochloride → HCID 87097842, compound

https://huagongshe.com/reaction/1617912

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66668182HCID 66668182—
ProductHCID 87097842HCID 87097842—

Reaction Steps

In analogy to example 151, step 3, 4-(1-(4-chloro-2-methylphenyl)-3-(1-methyl-6-oxo-1,6-dihydropyridin-3-yl)-3-oxopropyl)-N-(2-(methylsulfonyl)ethyl)benzamide was reacted with hydroxylamine hydrochloride in the presence of sodium hydrogencarbonate to give the title compound as a colourless solid, MS (ESI+): m/z=530.1 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-4691ecad050c4378b82b3afb732efa94
Source noteuspto-grants-2014_07