HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 67015651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Di-tert-butyl(2',4',6'-tris(propan-2-yl)-(1,1'-biphenyl)-2-yl)phosphane | HCID 11618717 | — |
| Reactant | HCID 66667222 | HCID 66667222 | — |
| Catalyst | Hexadecyltrimethylammonium Bromide | HCID 5974 | — |
| Catalyst | Bis(dibenzylideneacetone)palladium | HCID 9811564 | — |
| Product | HCID 67015651 | HCID 67015651 | — |
Reaction Steps
In analogy to example 364, step 1, from (S)-3-(4-bromo-phenyl)-3-(4-chloro-2-methyl-phenyl)-1-(2-methyl-pyridin-4-yl)-propan-1-one in presence of potassium hydroxide, 2-di-tert-butylphosphino-2′,4′,6′-triisopropylbiphenyl, tris(dibenzylideneacetone)dipalladium(0), cetyl trimethylammonium bromide and iodoethane was prepared the title compound as a yellow foam, MS (ESI+): m/z=394.0 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-210c7167ee6444ecaeb436251271f7c2 |
| Source note | uspto-grants-2014_07 |