HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136167027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 66668993 | HCID 66668993 | — |
| Product | HCID 136167027 | HCID 136167027 | — |
Reaction Steps
In analogy to example 132, step 6, from (3R)-3-(4-bromophenyl)-3-(4-chloro-2-methyl-phenyl)-2-methyl-1-(2-methylpyridin-4-yl)propan-1-one and hydroxylamine hydrochloride in the presence of sodium hydrogencarbonate was prepared the title compound as a white foam, MS (ESI+): m/z=457.0 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-54bd452c50874003b66ae278486de684 |
| Source note | uspto-grants-2014_07 |