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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617998Generated: November 3, 2026

Hydroxyamine hydrochloride → HCID 136166875, compound

https://huagongshe.com/reaction/1617998

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66666343HCID 66666343—
ProductHCID 136166875HCID 136166875—

Reaction Steps

In analogy to example 132, step 6, from (R)-3-(4-bromophenyl)-3-(4-chloro-2-methyl-phenyl)-1-(2-methylpyridin-4-yl)propan-1-one (example 282, step 1) and hydroxylamine hydrochloride in the presence of sodium hydrogencarbonate was prepared the title compound as a white foam, MS (ESI+): m/z=443.0 ([M+H]+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-2a992ee4f7b04fb3b85a410afa66ae38
Source noteuspto-grants-2014_07