HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Carboxyphenylboronic Acid → HCID 58043232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Carboxyphenylboronic Acid | HCID 312183 | — |
| Reactant | HCID 58043413 | HCID 58043413 | — |
| Product | HCID 58043232 | HCID 58043232 | — |
Reaction Steps
The title compound was prepared in analogy to example 166, from (E)-5-(3-(4-bromophenyl)-3-(2-fluoro-4-methylphenyl)-1-(hydroxyimino)propyl)-1-methylpyridin-2(1H)-one and 4-carboxyphenylboronic acid (CAS RN 14047-29-1). The compound was purified by silica gel chromatography using a MPLC system eluting with a gradient of dichloromethane:methanol (100:0 to 90:10). Yellow solid. MS (ESI+): m/z=485.2 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-7510c6dfd87e48f7ad90d74b000e474f |
| Source note | uspto-grants-2014_07 |