HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine → HCID 11269266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine | HCID 750 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 86595474 | HCID 86595474 | — |
| Product | HCID 11269266 | HCID 11269266 | — |
Reaction Steps
194 mg of 1-chloro-4-hydroxy-7-phenylsulfanyl-isoquinoline-3-carboxylic acid butyl ester (0.5 mmol) were reacted with glycine and sodium methylate analogously to Example D-1 g). 168 mg of the title compound were obtained; 1H NMR (DMSO-d6): δ=9.17 (t, 1H), 8.24 (d, 1H), 7.51 to 7.79 (m, 7 H), 4.00 (d, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765956B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e81c68adca854c2da22fb762bf4f2d12 |
| Source note | uspto-grants-2014_07 |